Electronic & Magnetic Materials & Devices Capabilities
Synthesis
Colloidal chemistry and self-assembly techniques
Complex oxide film synthesis via molecular beam epitaxy (DCA R450 Custom)
Physical vapor deposition (Lesker CMS 18 and PVD 250)
Spin coating (Laurell WS-400)
Characterization
Variable-temperature (VT) scanning tunneling microscope with atomic force microscopy capabilities (Omicron VT-AFM/STM), operates in an ultrahigh vacuum (UHV) environment with a base pressure of < 1E-10 mbar and 55-400 K. Atomic resolution is routinely obtained at room temperature and below. The AFM capabilities support a range of scanning modes. The analysis chamber also houses a LEED/Auger with an attached preparation chamber for sample cleaning and deposition (sputter cleaning, direct current heating, e-beam heating stage, metal deposition, etc.)
Variable-temperature scanning tunneling microscope (home-built VT-STM) operates in an UHV environment with a base pressure of < 1E-10 mbar and 55-300 K. Atomic resolution is routinely obtained at room temperature and below. The analysis chamber also houses a LEED/Auger with an attached preparation chamber for sample cleaning and deposition (sputter cleaning, direct current heating, e-beam heating stage, metal deposition).
Scanning probe microscope Veeco MultiMode 8 [contact or tapping mode, fluid imaging, low-current scanning tunneling microscopy, magnetic force microscopy, variable temperature imaging (-30-250°C), conductive atomic force microscopy, PeakForce tapping mode and PeakForce quantitative nanomechanical mapping]
Characterization of electrical transport properties at the nanoscale via state-of-the-art UHV nanoprobes (4-tip SEM Omicron UHV Nanoprobe)
Internal/external quantum efficiency measurement system (Oriel IQE-200)
Luminescence spectrometer (Perkin-Elmer LS 55)
Magnetic and physical properties characterization suite ( Keithley 4200-SCS/F Semiconductor Parameter Analyzer, Quantum Design PPMS-9 and MPMS XL)
Optical microscope (Zeiss Axio Imager Z1 M Upright)
The Center for Nanoscale Materials is an Office of Science User Facility operated for
the U.S.Department of Energy Office of Science by Argonne National Laboratory